Information card for entry 7009960

Structure parameters

• Formula: C27.5 H40 N O6 P Si2 W
• Calculated formula: C27.5 H40 N O6 P Si2 W
• Title of publication: Ferrocenium salt induced ring expansion of a 2H-azaphosphirene complex: Synthesis of the first Δ3-1,4,2-oxazaphospholene complexes †
• Authors of publication: Streubel, Rainer; Neumann, Christoph; Jones, Peter G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 15
• Pages of publication: 2495
• a: 36.058 ± 0.004 Å
• b: 10.4819 ± 0.0012 Å
• c: 19.602 ± 0.002 Å
• α: 90°
• β: 119.33 ± 0.006°
• γ: 90°
• Cell volume: 6459 ± 1.3 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0413
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0523
• Weighted residual factors for all reflections included in the refinement: 0.0589
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No