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Information card for entry 7009963
Preview
Coordinates | 7009963.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32.5 H47 K2 N2 O17 |
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Calculated formula | C32.5 H47 K2 N2 O17 |
Title of publication | N-Glycosylamines of 4,6-O-ethylidene-α-D-glucopyranose: synthesis, characterisation and structure of CO2H, Cl and F ortho-substituted phenyl derivatives and metal ion complexes of the CO2H derivative† |
Authors of publication | Sah, Ajay K.; Rao, Chebrolu P.; Saarenketo, Pauli K.; Wegelius, Elina K.; Rissanen, Kari; Kolehmainen, Erkki |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2000 |
Journal issue | 20 |
Pages of publication | 3681 |
a | 21.562 ± 0.001 Å |
b | 13.501 ± 0.001 Å |
c | 15.041 ± 0.001 Å |
α | 90° |
β | 122.07 ± 0.01° |
γ | 90° |
Cell volume | 3710.4 ± 0.6 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0439 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for all reflections | 0.0983 |
Weighted residual factors for significantly intense reflections | 0.0943 |
Goodness-of-fit parameter for all reflections | 1.106 |
Goodness-of-fit parameter for significantly intense reflections | 1.114 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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