Information card for entry 7010102

Structure parameters

• Formula: C44 H45 Cl4 O2 P2 Re2
• Calculated formula: C44 H45 Cl4 O2 P2 Re2
• Title of publication: Reactions of the dirhenium(III,III) complex cis-Re2(μ-O2CMe)2Cl4(H2O)2 that lead to the dirhenium(III,II) complexes Re2(μ-O2CMe)Cl4(PR3)2 and tetrarheniumcyclodiyne clusters of the type Re4(μ-O)4Cl4(PR3)4
• Authors of publication: Bera, Jitendra K.; Lau, Sophia S.; Fanwick, Phillip E.; Walton, Richard A.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4277
• a: 9.8942 ± 0.0005 Å
• b: 13.5625 ± 0.0009 Å
• c: 18.4975 ± 0.0012 Å
• α: 69.437 ± 0.003°
• β: 76.902 ± 0.004°
• γ: 69.586 ± 0.003°
• Cell volume: 2162.7 ± 0.2 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for all reflections included in the refinement: 0.099
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No