Information card for entry 7010106

Structure parameters

• Formula: C44 H48 Cl8 O6 P2 Re2
• Calculated formula: C44 H48 Cl8 O6 P2 Re4
• Title of publication: Reactions of the dirhenium(III,III) complex cis-Re2(μ-O2CMe)2Cl4(H2O)2 that lead to the dirhenium(III,II) complexes Re2(μ-O2CMe)Cl4(PR3)2 and tetrarheniumcyclodiyne clusters of the type Re4(μ-O)4Cl4(PR3)4
• Authors of publication: Bera, Jitendra K.; Lau, Sophia S.; Fanwick, Phillip E.; Walton, Richard A.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4277
• a: 16.5256 ± 0.0003 Å
• b: 18.6675 ± 0.0004 Å
• c: 33.0129 ± 0.0004 Å
• α: 90°
• β: 100.512 ± 0.0011°
• γ: 90°
• Cell volume: 10013.3 ± 0.3 ų
• Cell temperature: 193 K
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for all reflections included in the refinement: 0.122
• Goodness-of-fit parameter for all reflections included in the refinement: 0.946
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No