Information card for entry 7010185

Structure parameters

• Formula: C23 H6 O11 Os3 S2
• Calculated formula: C23 H6 O11 Os3 S2
• Title of publication: A new two-strand chain cluster: the synthesis and characterisation of [Os3(CO)11{μ3-η4-(C4H3S)C2C2(C4H3S)}] †
• Authors of publication: Adams, Christopher J.; Clarke, Lionel P.; Martín-Castro, Ana M.; Raithby, Paul R.; Shields, Gregory P.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 22
• Pages of publication: 4015
• a: 7.071 ± 0.004 Å
• b: 21.964 ± 0.012 Å
• c: 16.564 ± 0.01 Å
• α: 90°
• β: 96.15 ± 0.04°
• γ: 90°
• Cell volume: 2558 ± 3 ų
• Cell temperature: 195 ± 2 K
• Ambient diffraction temperature: 195 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.0626
• Weighted residual factors for all reflections: 0.1766
• Weighted residual factors for significantly intense reflections: 0.1665
• Goodness-of-fit parameter for all reflections: 1.059
• Goodness-of-fit parameter for significantly intense reflections: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No