Information card for entry 7010213

Structure parameters

• Formula: C32 H38 N4 Sb2
• Calculated formula: C32 H38 N4 Sb2
• SMILES: c1c(C)c(N[Sb]2N(c3c(cccc3C)C)[Sb](Nc3c(cccc3C)C)N2c2c(cccc2C)C)c(cc1)C
• Title of publication: Antimony imido and imido‒amido compounds: a new route to an imidoantimony macrocycle
• Authors of publication: Bryant, Richard; James, Siân C.; Jeffery, John C.; Norman, Nicholas C.; Orpen, A. Guy; Weckenmann, Ulrike
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 22
• Pages of publication: 4007
• a: 7.9276 ± 0.0019 Å
• b: 10.012 ± 0.003 Å
• c: 11.075 ± 0.004 Å
• α: 101 ± 0.02°
• β: 110.705 ± 0.014°
• γ: 107.892 ± 0.014°
• Cell volume: 736.9 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0684
• Weighted residual factors for all reflections included in the refinement: 0.0735
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No