Crystallography Open Database

Information card for entry 7010223

Preview

Coordinates	7010223.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18.5 H2.5 Cl1.5 O18 Os3 Re2 S
Calculated formula	C18.5 H Cl1.5 O18 Os3 Re2 S
Title of publication	The syntheses of novel sulfur centred spirocyclic cluster complexes starting from [Re2(μ-H)(μ-SH)(CO)8]
Authors of publication	Egold, Hans; Schwarze, Detlef; Schraa, Markus; Flörke, Ulrich
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	23
Pages of publication	4385
a	35.48 ± 0.009 Å
b	11.534 ± 0.002 Å
c	16.023 ± 0.006 Å
α	90°
β	111.67 ± 0.02°
γ	90°
Cell volume	6094 ± 3 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0772
Residual factor for significantly intense reflections	0.0424
Weighted residual factors for significantly intense reflections	0.0784
Weighted residual factors for all reflections included in the refinement	0.09
Goodness-of-fit parameter for all reflections included in the refinement	0.966
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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