Information card for entry 7010258

Structure parameters

• Formula: C54 H77 Cl6 N O12 Rh2
• Calculated formula: C54 H77 Cl6 N O12 Rh2
• Title of publication: Dirhodium(II) carboxylates as building blocks. Synthesis and structures of cis-chelate complexes
• Authors of publication: Bonar-Law, Richard P.; McGrath, Thomas D.; Singh, Nirmal; Bickley, Jamie F.; Femoni, Cristina; Steiner, Alexander
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4343
• a: 17.918 ± 0.003 Å
• b: 9.4795 ± 0.0007 Å
• c: 36.978 ± 0.004 Å
• α: 90°
• β: 90.107 ± 0.016°
• γ: 90°
• Cell volume: 6280.8 ± 1.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.116
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.133
• Weighted residual factors for all reflections included in the refinement: 0.1547
• Goodness-of-fit parameter for all reflections included in the refinement: 0.748
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No