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Information card for entry 7010260
Preview
Coordinates | 7010260.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C38.5 H31.5 Cl2 N3 O2 Os P |
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Calculated formula | C38.5 H31.5 Cl2 N3 O2 Os P |
Title of publication | Cyclometallation and NN bond cleavage of 2-(arylazo)phenols by osmium. Synthesis, structure and redox properties † |
Authors of publication | Majumder, Kanchana; Peng, Shie-Ming; Bhattacharya, Samaresh |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2001 |
Journal issue | 3 |
Pages of publication | 284 |
a | 40.4327 ± 0.0002 Å |
b | 10.9195 ± 0.0002 Å |
c | 17.5688 ± 0.0003 Å |
α | 90° |
β | 112.731 ± 0.001° |
γ | 90° |
Cell volume | 7154.24 ± 0.19 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 7 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0835 |
Residual factor for significantly intense reflections | 0.0564 |
Weighted residual factors for all reflections | 0.1456 |
Weighted residual factors for significantly intense reflections | 0.1353 |
Goodness-of-fit parameter for all reflections | 1.021 |
Goodness-of-fit parameter for significantly intense reflections | 1.117 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7010260.html
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