Information card for entry 7010274

Structure parameters

• Formula: C124 H164 O26 Rh4
• Calculated formula: C124 H164 O26 Rh4
• Title of publication: Dirhodium(II) carboxylates as building blocks. Macrocyclic dimers with vertically stacked Rh24+ units
• Authors of publication: Bonar-Law, Richard P.; Bickley, Jamie F.; Femoni, Cristina; Steiner, Alexander
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4244
• a: 14.36 ± 0.004 Å
• b: 24.341 ± 0.004 Å
• c: 19.477 ± 0.005 Å
• α: 90°
• β: 99.01 ± 0.03°
• γ: 90°
• Cell volume: 6724 ± 3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1179
• Residual factor for significantly intense reflections: 0.0674
• Weighted residual factors for significantly intense reflections: 0.1782
• Weighted residual factors for all reflections included in the refinement: 0.209
• Goodness-of-fit parameter for all reflections included in the refinement: 0.974
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No