Information card for entry 7010288

Structure parameters

• Formula: C33 H33 Cl Cu P
• Calculated formula: C33 H33 Cl Cu P
• Title of publication: Structural and spectroscopic studies on three- and two-co-ordinate copper(I) halide tribenzylphosphine complexes
• Authors of publication: Ainscough, Eric W.; Brodie, Andrew M.; Burrell, Anthony K.; Freeman, Graham H.; Jameson, Geoffrey B.; Bowmaker, Graham A.; Hanna, John V.; Healy, Peter C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 2
• Pages of publication: 144
• a: 9.902 ± 0.003 Å
• b: 10.432 ± 0.004 Å
• c: 14.326 ± 0.005 Å
• α: 94.71 ± 0.005°
• β: 97.485 ± 0.004°
• γ: 95.759 ± 0.005°
• Cell volume: 1453 ± 0.9 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0933
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1187
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No