Information card for entry 7010303

Structure parameters

• Formula: C32 H56 N6 O P2
• Calculated formula: C31.962 H56.666 N6 O P2
• Title of publication: Titanium complexes of bis(1°-amido)cyclodiphosph(III)azanes and bis(1°-amido)cyclodiphosph(V)azanes: facial versus lateral coordination †
• Authors of publication: Moser, Daniel F.; Carrow, Christopher J.; Stahl, Lothar; Staples, Richard J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 8
• Pages of publication: 1246
• a: 9.882 ± 0.002 Å
• b: 10.931 ± 0.002 Å
• c: 18.481 ± 0.004 Å
• α: 89.14 ± 0.03°
• β: 78.07 ± 0.03°
• γ: 68.42 ± 0.03°
• Cell volume: 1812.2 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1414
• Residual factor for significantly intense reflections: 0.1051
• Weighted residual factors for significantly intense reflections: 0.2203
• Weighted residual factors for all reflections included in the refinement: 0.2424
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No