Information card for entry 7010306

Structure parameters

• Formula: C23 H45 Cl3 N4 P2 S2 Ti
• Calculated formula: C23 H37 Cl3 N4 P2 S2 Ti
• Title of publication: Titanium complexes of bis(1°-amido)cyclodiphosph(III)azanes and bis(1°-amido)cyclodiphosph(V)azanes: facial versus lateral coordination †
• Authors of publication: Moser, Daniel F.; Carrow, Christopher J.; Stahl, Lothar; Staples, Richard J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 8
• Pages of publication: 1246
• a: 9.1295 ± 0.001 Å
• b: 13.4498 ± 0.0014 Å
• c: 14.1424 ± 0.0014 Å
• α: 90°
• β: 94.488 ± 0.009°
• γ: 90°
• Cell volume: 1731.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0684
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1279
• Weighted residual factors for all reflections included in the refinement: 0.139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No