Information card for entry 7010327

Structure parameters

• Chemical name: Tetrakis(tetraamminelithium)nonaplumbide-ammonia(1/1)
• Formula: H51 Li4 N17 Pb9
• Calculated formula: H51 Li4 N17 Pb9
• SMILES: [Pb]123[Pb]456[Pb]789[Pb]%10([Pb]257)[Pb]258[Pb]14([Pb]3%102)[Pb]695.[NH3][Li]([NH3])([NH3])[NH3].[NH3][Li]([NH3])([NH3])[NH3].[NH3][Li]([NH3])([NH3])[NH3].[NH3][Li]([NH3])([NH3])[NH3].N
• Title of publication: Synthesis and crystal structure of [Li(NH3)4]4[Sn9]·NH3 and [Li(NH3)4]4[Pb9]·NH3 †
• Authors of publication: Korber, Nikolaus; Fleischmann, Andrea
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 383
• a: 10.6109 ± 0.0008 Å
• b: 17.8636 ± 0.0009 Å
• c: 21.4144 ± 0.0016 Å
• α: 90°
• β: 99.046 ± 0.009°
• γ: 90°
• Cell volume: 4008.6 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0767
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0685
• Weighted residual factors for all reflections included in the refinement: 0.0753
• Goodness-of-fit parameter for all reflections included in the refinement: 0.909
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No