Information card for entry 7010334

Structure parameters

• Common name: Tris(tetra-n-butylammonium) trihydrogendecavanadate
• Formula: C48 H111 N3 O28 V10
• Calculated formula: C48 H111 N3 O28 V10
• Title of publication: Hydrogen-bonded aggregates of protonated decavanadate anions in their tetraalkylammonium salts † ‡
• Authors of publication: Nakamura, Setsuko; Ozeki, Tomoji
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 472
• a: 15.968 ± 0.002 Å
• b: 18.677 ± 0.002 Å
• c: 12.785 ± 0.002 Å
• α: 91.38 ± 0.01°
• β: 96.48 ± 0.01°
• γ: 107.26 ± 0.01°
• Cell volume: 3611.3 ± 0.8 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.154
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1777
• Weighted residual factors for all reflections included in the refinement: 0.2678
• Goodness-of-fit parameter for all reflections included in the refinement: 0.939
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No