Information card for entry 7010360

Structure parameters

• Formula: C48 H58 O4 P2 Pd
• Calculated formula: C48 H56 O4 P2 Pd
• Title of publication: A new chiral metalladiphosphine for early‒late chemistry. Crystal structure of a D-camphor-based zirconium enolato phosphine and rearrangement of heterobimetallic Zr/Pd complexes †
• Authors of publication: Mattheis, Chris; Braunstein, Pierre; Fischer, Axel
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 6
• Pages of publication: 800
• a: 10.484 ± 0.0002 Å
• b: 34.061 ± 0.0007 Å
• c: 12.962 ± 0.0002 Å
• α: 90°
• β: 112.67 ± 0.003°
• γ: 90°
• Cell volume: 4271.06 ± 0.17 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.037
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for all reflections: 0.222
• Weighted residual factors for all reflections included in the refinement: 0.035
• Goodness-of-fit parameter for all reflections: 6.686
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No