Information card for entry 7010374

Structure parameters

• Formula: C26 H39 N10 Ni2 O2.5
• Calculated formula: C26 H38 N10 Ni2 O3
• Title of publication: Novel nickel(II) complexes with diazamesocyclic ligands functionalized by additional phenol donor pendant(s): synthesis, characterization, crystal structures and magnetic properties
• Authors of publication: Bu, Xian-He; Du, Miao; Zhang, Lei; Liao, Dai-Zheng; Tang, Jin-Kui; Zhang, Ruo-Hua; Shionoya, Mitsuhiko
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 593
• a: 13.311 ± 0.002 Å
• b: 16.542 ± 0.003 Å
• c: 13.407 ± 0.002 Å
• α: 90°
• β: 98.851 ± 0.004°
• γ: 90°
• Cell volume: 2916.9 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.105
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1343
• Weighted residual factors for all reflections included in the refinement: 0.1561
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No