Information card for entry 7010384

Structure parameters

• Formula: C11 H23 Cl2 Co N4 O14
• Calculated formula: C11 H23 Cl2 Co N4 O14
• Title of publication: Preparation, structures and reactions of isomeric [Co(cyclen)(O2C2O2)]+ and [Co(cyclen)(O2CCH2CO2)]+ complexes (cyclen = 1,4,7,10-tetraazacyclododecane) †
• Authors of publication: Clarkson, Andrea J.; Blackman, Allan G.; Clark, Charles R.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 758
• a: 18.022 ± 0.004 Å
• b: 14.943 ± 0.003 Å
• c: 32.02 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8623 ± 3 ų
• Cell temperature: 168 ± 2 K
• Ambient diffraction temperature: 168 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1033
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.0953
• Weighted residual factors for all reflections included in the refinement: 0.1128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No