Information card for entry 7010421

Structure parameters

• Formula: C16 H29 Li N2 O4 Si
• Calculated formula: C16 H29 Li N2 O4 Si
• SMILES: [Li]1234([n]5ccccc5N1[Si](C)(C)C)[O]1CC[O]2CC[O]3CC[O]4CC1
• Title of publication: Cation-induced structural variations in the alkali metal derivatives of 2-trimethylsilylaminopyridine: synthesis and X-ray structures of complexes for all five metals Li‒Cs with 12-crown-4 †
• Authors of publication: Liddle, Stephen T.; Clegg, William
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 402
• a: 9.9095 ± 0.0003 Å
• b: 12.2197 ± 0.0004 Å
• c: 16.2582 ± 0.0005 Å
• α: 90°
• β: 99.935 ± 0.002°
• γ: 90°
• Cell volume: 1939.2 ± 0.11 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0303
• Residual factor for significantly intense reflections: 0.0277
• Weighted residual factors for significantly intense reflections: 0.0733
• Weighted residual factors for all reflections included in the refinement: 0.0749
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No