Information card for entry 7010432

Structure parameters

• Formula: C32 H38 B N6 P Ru S3
• Calculated formula: C32 H38 B N6 P Ru S3
• Title of publication: Synthesis and characterisation of a series of ruthenium scorpionate complexes with B‒HM agostic interactions. Crystal structure of [RuH(κ2-N,BH TpTn)(PMe3)(cod)] (TpTn = hydrotris[3-(2-thienyl)pyrazol-1-yl]borate)
• Authors of publication: Agustín Caballero; Felipe Gómezde la Torre; Félix A. Jalón; Blanca R. Manzano; Ana M. Rodríguez; Swiatoslaw Trofimenko; Michael P. Sigalas
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 427 - 433
• a: 10.682 ± 0.005 Å
• b: 11.427 ± 0.005 Å
• c: 14.375 ± 0.005 Å
• α: 97.02 ± 0.005°
• β: 105.6 ± 0.005°
• γ: 94.07 ± 0.005°
• Cell volume: 1667.4 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0883
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.1069
• Weighted residual factors for all reflections included in the refinement: 0.1503
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No