Information card for entry 7010445

Structure parameters

• Formula: C28.5 H27.5 Cl3.5 N O3 P2 Pd
• Calculated formula: C28.5 H27.5 Cl3.5 N O3 P2 Pd
• Title of publication: Novel chiral phosphine ligands and complexes from amino acid esters
• Authors of publication: Slawin, Alexandra M. Z.; Woollins, J. Derek; Zhang, Qingzhi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 621
• a: 12.3753 ± 0.0002 Å
• b: 16.1471 ± 0.0004 Å
• c: 17.4554 ± 0.0001 Å
• α: 90°
• β: 108.893 ± 0.001°
• γ: 90°
• Cell volume: 3300.11 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1131
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for all reflections: 0.2681
• Weighted residual factors for significantly intense reflections: 0.2083
• Goodness-of-fit parameter for all reflections: 1.138
• Goodness-of-fit parameter for significantly intense reflections: 1.236
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No