Information card for entry 7010450

Structure parameters

• Formula: C34 H45 Cl7 N2 P2 Si2 Zr
• Calculated formula: C34 H45 Cl7 N2 P2 Si2 Zr
• Title of publication: The reactivity of trimethylsilyliminophosphines towards titanium and zirconium halides
• Authors of publication: Sarsfield, Mark J.; Said, Musa; Thornton-Pett, Mark; Gerrard, Lee A.; Bochmann, Manfred
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 6
• Pages of publication: 822
• a: 22.676 ± 0.001 Å
• b: 9.5021 ± 0.0005 Å
• c: 21.3807 ± 0.0007 Å
• α: 90°
• β: 113.031 ± 0.003°
• γ: 90°
• Cell volume: 4239.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1608
• Residual factor for significantly intense reflections: 0.1024
• Weighted residual factors for significantly intense reflections: 0.2
• Weighted residual factors for all reflections included in the refinement: 0.2288
• Goodness-of-fit parameter for all reflections included in the refinement: 1.198
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No