Information card for entry 7010471

Structure parameters

• Formula: C20 H18 Gd2 O19 S4
• Calculated formula: C20 H12 Gd2 O19 S4
• Title of publication: In situ ligand synthesis and the first crystallographically characterized lanthanide 3-D pillared networks containing benzene-1,4-disulfonate as a building block †
• Authors of publication: Xiong, Ren-Gen; Zhang, Jing; Chen, Zhen-Feng; You, Xiao-Zeng; Che, Chi-Ming; Fun, Hoong-Kun
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 6
• Pages of publication: 780
• a: 15.855 ± 0.002 Å
• b: 20.492 ± 0.003 Å
• c: 8.1388 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2644.3 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0965
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.2598
• Weighted residual factors for all reflections included in the refinement: 0.2649
• Goodness-of-fit parameter for all reflections included in the refinement: 2.125
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No