Information card for entry 7010476

Structure parameters

• Formula: C180 H192 N32 O32 Rh8
• Calculated formula: C180 H185.854 N32 O32 Rh8
• Title of publication: Supramolecular squares with Rh24+ corners
• Authors of publication: Cotton, F. Albert; Daniels, Lee M.; Lin, Chun; Murillo, Carlos A.; Yu, Shu-Yan
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 502
• a: 14.2593 ± 0.0004 Å
• b: 18.608 ± 0.005 Å
• c: 20.147 ± 0.003 Å
• α: 80.59 ± 0.02°
• β: 75.51 ± 0.01°
• γ: 71.45 ± 0.01°
• Cell volume: 4886.3 ± 1.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0765
• Residual factor for significantly intense reflections: 0.0626
• Weighted residual factors for all reflections: 0.1608
• Weighted residual factors for significantly intense reflections: 0.1412
• Goodness-of-fit parameter for all reflections: 1.142
• Goodness-of-fit parameter for significantly intense reflections: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No