Information card for entry 7010479

Structure parameters

• Formula: C176 H173 Cl4 N27 O32 Rh8
• Calculated formula: C176 Cl4 N27 O32 Rh8
• Title of publication: Supramolecular squares with Rh24+ corners
• Authors of publication: Cotton, F. Albert; Daniels, Lee M.; Lin, Chun; Murillo, Carlos A.; Yu, Shu-Yan
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 502
• a: 14.681 ± 0.003 Å
• b: 18.661 ± 0.003 Å
• c: 20.742 ± 0.004 Å
• α: 77.818 ± 0.003°
• β: 75.205 ± 0.004°
• γ: 74.44 ± 0.003°
• Cell volume: 5230.4 ± 1.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1977
• Residual factor for significantly intense reflections: 0.1639
• Weighted residual factors for significantly intense reflections: 0.4847
• Weighted residual factors for all reflections included in the refinement: 0.5163
• Goodness-of-fit parameter for all reflections included in the refinement: 2.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No