Information card for entry 7010516

Structure parameters

• Formula: C42 H43 B Cl10 F6 N6 O2 P2 Rh
• Calculated formula: C42 H43 B Cl10 F6 N6 O2 P2 Rh
• Title of publication: Redox-active catecholate complexes of rhodium hydrotris(pyrazolyl)borates
• Authors of publication: Connelly, Neil G.; Emslie, David J. H.; Hayward, Owen D.; Orpen, A. Guy; Quayle, Michael J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 6
• Pages of publication: 875
• a: 26.1501 ± 0.0013 Å
• b: 13.756 ± 0.003 Å
• c: 14.6012 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5252.4 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.0435
• Weighted residual factors for significantly intense reflections: 0.1084
• Weighted residual factors for all reflections included in the refinement: 0.1153
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No