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Information card for entry 7010544
Preview
Coordinates | 7010544.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H24 B Cl10 F13 P Rh S |
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Calculated formula | C32 H24 B Cl10 F13 P Rh S |
Title of publication | Intramolecular SNAr reactions as a route to complexes of hybrid cyclopentadienyl‒phosphine ligands: synthesis of a rhodium complex of the first η5,η1,η1-cyclopentadienyl‒phosphine‒thioether ligand |
Authors of publication | Bellabarba, Ronan M.; Nieuwenhuyzen, Mark; Saunders, Graham C. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2001 |
Journal issue | 5 |
Pages of publication | 512 |
a | 11.6484 ± 0.0009 Å |
b | 11.7516 ± 0.001 Å |
c | 17.7351 ± 0.0014 Å |
α | 93.233 ± 0.002° |
β | 102.549 ± 0.001° |
γ | 112.306 ± 0.001° |
Cell volume | 2166.3 ± 0.3 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0701 |
Residual factor for significantly intense reflections | 0.047 |
Weighted residual factors for significantly intense reflections | 0.11 |
Weighted residual factors for all reflections included in the refinement | 0.1204 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.935 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7010544.html
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