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Information card for entry 7010581
Preview
Coordinates | 7010581.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H48 B9 N3 W |
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Calculated formula | C21 H47 B9 N3 W |
Title of publication | Tungsten(VI) metallacarborane imido complexes; hydrogen bonding to a bent imido ligand in {W(NtBu)2[N(H)C(Me)NHtBu](C2B9H11)} † |
Authors of publication | Batsanov, Andrei S.; Goeta, Andrés E.; Howard, Judith A. K.; Hughes, Andrew K.; Johnson, Andrew L.; Wade, Ken |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2001 |
Journal issue | 8 |
Pages of publication | 1210 |
a | 11.404 ± 0.001 Å |
b | 11.501 ± 0.001 Å |
c | 22.696 ± 0.001 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2976.7 ± 0.4 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0273 |
Residual factor for significantly intense reflections | 0.0237 |
Weighted residual factors for all reflections | 0.0603 |
Weighted residual factors for significantly intense reflections | 0.0543 |
Goodness-of-fit parameter for all reflections | 1.14 |
Goodness-of-fit parameter for significantly intense reflections | 1.091 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7010581.html
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