Information card for entry 7010653

Structure parameters

• Formula: C32.25 H30.25 Cl4.25 N O0.75 P2 Pt S0.75
• Calculated formula: C32.25 H30.25 Cl4.25 N O0.75 P2 Pt S0.75
• Title of publication: Synthesis of chelate complexes and the dichalcogen derivatives of the unsymmetrical diphosphine ligand Ph2PNHC6H4PPh2. Molecular structure of [PtCl2(Ph2PNHC6H4PPh2)]·0.75dmso·0.75CHCl3
• Authors of publication: Aucott, Stephen M.; Slawin, Alexandra M. Z.; Woollins, J. Derek
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 15
• Pages of publication: 2279
• a: 12.2267 ± 0.0002 Å
• b: 21.7198 ± 0.0003 Å
• c: 14.1548 ± 0.0002 Å
• α: 90°
• β: 98.806 ± 0.001°
• γ: 90°
• Cell volume: 3714.66 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0396
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for all reflections: 0.1088
• Weighted residual factors for significantly intense reflections: 0.0893
• Goodness-of-fit parameter for all reflections: 1.04
• Goodness-of-fit parameter for significantly intense reflections: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No