Information card for entry 7010663

Structure parameters

• Formula: C12 H36 Cl3 Ir2 N6 O12 S6 V
• Calculated formula: C12 H36 Cl3 Ir2 N6 O12 S6 V
• Title of publication: Synthesis, characterization and reactivity of linear-type S-bridged trinuclear complexes containing vanadium(III) ion. Crystal structures of [VIII{M(aet)3}2](ClO4)3 (M = RhIII, IrIII; aet = 2-aminoethanethiolate)†
• Authors of publication: Miyashita, Yoshitaro; Hamajima, Masato; Yamada, Yasunori; Fujisawa, Kiyoshi; Okamoto, Ken-ichi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 14
• Pages of publication: 2089
• a: 14.578 ± 0.009 Å
• b: 14.578 ± 0.009 Å
• c: 26.47 ± 0.02 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4872 ± 6 ų
• Cell temperature: 296.2 K
• Number of distinct elements: 8
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for all reflections included in the refinement: 0.0474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.36
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No