Information card for entry 7010682

Structure parameters

• Formula: C12 H36 Co2 N8 S8 Sb4
• Calculated formula: C12 H36 Co2 N8 S8 Sb4
• Title of publication: Thioantimonate(III) anions acting as bridging ligands in neutral transition metal complexes: solvothermal synthesis and characterisation of the two novel compounds [Co(C6H18N4)]2Sb4S8 and [Co(C6H18N4)]2Sb2S5 containing [Sb4S8]4‒ and [Sb2S5]4‒ anions
• Authors of publication: Stähler, Ralph; Bensch, Wolfgang
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 17
• Pages of publication: 2518
• a: 17.936 ± 0.004 Å
• b: 13.442 ± 0.003 Å
• c: 14 ± 0.003 Å
• α: 90°
• β: 101.73 ± 0.03°
• γ: 90°
• Cell volume: 3304.9 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0369
• Residual factor for significantly intense reflections: 0.0236
• Weighted residual factors for significantly intense reflections: 0.0521
• Weighted residual factors for all reflections included in the refinement: 0.055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No