Information card for entry 7010723

Structure parameters

• Formula: C14 H72 Cu4 N14 O68 P2 W17
• Calculated formula: C14 H72 Cu4 N14 O68 P2 W17
• Title of publication: Hydrothermal syntheses and structures of three one-dimensional heteropolytungstates formed by Dawson or Keggin cluster units
• Authors of publication: Yan, Bangbo; Xu, Yan; Bu, Xianhui; Goh, Ngoh K.; Chia, Lian S.; Stucky, Galen D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 13
• Pages of publication: 2009
• a: 11.71 ± 0.004 Å
• b: 13.228 ± 0.004 Å
• c: 28.161 ± 0.008 Å
• α: 90.576 ± 0.016°
• β: 95.76 ± 0.02°
• γ: 112.525 ± 0.019°
• Cell volume: 4003 ± 2 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1117
• Residual factor for significantly intense reflections: 0.0653
• Weighted residual factors for significantly intense reflections: 0.1425
• Weighted residual factors for all reflections included in the refinement: 0.1573
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No