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Information card for entry 7010747
Preview
Coordinates | 7010747.cif |
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Original paper (by DOI) | HTML |
Common name | NacNacLi(Et2O) |
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Formula | C33 H51 Li N2 O |
Calculated formula | C33 H51 Li N2 O |
Title of publication | The synthesis and structure of lithium derivatives of the sterically encumbered β-diketiminate ligand [{(2,6-Pri2H3C6)N(CH3)C}2CH]‒, and a modified synthesis of the aminoimine precursor |
Authors of publication | Stender, Matthias; Wright, Robert J.; Eichler, Barrett E.; Prust, Jörg; Olmstead, Marilyn M.; Roesky, Herbert W.; Power, Philip P. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2001 |
Journal issue | 23 |
Pages of publication | 3465 |
a | 47.323 ± 0.006 Å |
b | 10.1697 ± 0.0009 Å |
c | 19.9329 ± 0.0012 Å |
α | 90° |
β | 94.366 ± 0.007° |
γ | 90° |
Cell volume | 9565.1 ± 1.6 Å3 |
Cell temperature | 140 ± 2 K |
Ambient diffraction temperature | 140 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0601 |
Residual factor for significantly intense reflections | 0.0474 |
Weighted residual factors for significantly intense reflections | 0.1213 |
Weighted residual factors for all reflections included in the refinement | 0.1313 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.999 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7010747.html
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