Information card for entry 7010795

Structure parameters

• Formula: C32 H64 Cu2 N2 Si6
• Calculated formula: C32 H64 Cu2 N2 Si6
• Title of publication: Syntheses and crystal structures of binuclear gold(I), silver(I) and copper(I) complexes containing bulky pyridyl functionalised alkyl ligands
• Authors of publication: Tania R. van den Ancker; Suresh K. Bhargava; Fabian Mohr; Stavroula Papadopoulos; Colin L. Raston; Brian W. Skelton; Allan H. White
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2001
• Journal issue: 20
• Pages of publication: 3069 - 3072
• a: 12.156 ± 0.005 Å
• b: 20.98 ± 0.01 Å
• c: 18.848 ± 0.006 Å
• α: 90°
• β: 110.78 ± 0.03°
• γ: 90°
• Cell volume: 4494 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for all reflections: 0.055
• Weighted residual factors for all reflections included in the refinement: 0.051
• Goodness-of-fit parameter for all reflections: 1.675
• Goodness-of-fit parameter for all reflections included in the refinement: 1.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No