Information card for entry 7010805

Structure parameters

• Formula: C26 H2 Al2 Cl6 F55 O6 P
• Calculated formula: C26 H2 Al2 Cl6 F55 O6 P
• Title of publication: Reactions of P4 and I2 with Ag[Al(OC(CF3)3)4]: from elusive polyphosphorus cations to subvalent P3I6+ and phosphorus rich P5I2+
• Authors of publication: Ingo Krossing
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 500 - 512
• a: 12.781 ± 0.003 Å
• b: 13.445 ± 0.003 Å
• c: 16.561 ± 0.003 Å
• α: 88.45 ± 0.03°
• β: 69.56 ± 0.03°
• γ: 82.99 ± 0.03°
• Cell volume: 2646.4 ± 1.1 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1497
• Residual factor for significantly intense reflections: 0.1298
• Weighted residual factors for significantly intense reflections: 0.3729
• Weighted residual factors for all reflections included in the refinement: 0.3932
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No