Information card for entry 7010815

Structure parameters

• Formula: C44 H73 Eu F12 O13 Zr2
• Calculated formula: C44 H58 Eu F12 O13 Zr2
• Title of publication: Reactivity of the europium hexafluoroacetylacetonate (hfac) complex, Eu(hfac)3(diglyme), and related analogs with potassium: formation of the fluoride hfac “ate” complexes, [LnF(hfac)3K(diglyme)]2
• Authors of publication: William J. Evans; Dimitrios G. Giarikos; Matthew A. Johnston; Michael A. Greci; Joseph W. Ziller
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 520 - 526
• a: 16.6625 ± 0.0009 Å
• b: 21.3117 ± 0.0011 Å
• c: 16.4412 ± 0.0008 Å
• α: 90°
• β: 100.911 ± 0.001°
• γ: 90°
• Cell volume: 5732.8 ± 0.5 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1349
• Weighted residual factors for all reflections included in the refinement: 0.1398
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No