Information card for entry 7010854

Structure parameters

• Formula: C35 H46 Cl2 N3 O1.5 P Rh
• Calculated formula: C35 H39 Cl2 N3 O1.5 P Rh
• Title of publication: Synthesis and structure of novel rhodium complexes of multi-functionalised amine-phosphine ligands
• Authors of publication: Clarke, Matthew L.; Slawin, Alexandra M. Z.; Wheatley, Matthew V.; Woollins, J. Derek
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 23
• Pages of publication: 3421
• a: 13.0569 ± 0.0003 Å
• b: 19.4344 ± 0.0005 Å
• c: 13.9166 ± 0.0003 Å
• α: 90°
• β: 91.135 ± 0.001°
• γ: 90°
• Cell volume: 3530.69 ± 0.14 ų
• Cell temperature: 566 ± 2 K
• Ambient diffraction temperature: 566 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for all reflections: 0.1928
• Weighted residual factors for significantly intense reflections: 0.1414
• Goodness-of-fit parameter for all reflections: 1.126
• Goodness-of-fit parameter for significantly intense reflections: 1.22
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No