Information card for entry 7010856

Structure parameters

• Formula: C31 H41 Cl2 N3 O5 P Rh
• Calculated formula: C31 H41 Cl2 N3 O5 P Rh
• Title of publication: Synthesis and structure of novel rhodium complexes of multi-functionalised amine-phosphine ligands
• Authors of publication: Clarke, Matthew L.; Slawin, Alexandra M. Z.; Wheatley, Matthew V.; Woollins, J. Derek
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 23
• Pages of publication: 3421
• a: 16.6792 ± 0.0011 Å
• b: 9.7256 ± 0.0006 Å
• c: 21.2011 ± 0.0013 Å
• α: 90°
• β: 97.336 ± 0.001°
• γ: 90°
• Cell volume: 3411 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0831
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for all reflections: 0.104
• Weighted residual factors for significantly intense reflections: 0.082
• Goodness-of-fit parameter for all reflections: 0.95
• Goodness-of-fit parameter for significantly intense reflections: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No