Information card for entry 7010861

Structure parameters

• Formula: C46 H80 K2 O4 P2
• Calculated formula: C46 H80 K2 O4 P2
• Title of publication: Syntheses and solid-state structures of [{K(THF)2(PHTipp)K(THF)(μ-THF)(PHTipp)}x]2 and [Rb(THF)(PHTipp)]x (Tipp = 2,4,6-Pri3C6H2)
• Authors of publication: Christoph Frenzel; Fernando Somoza Jr.; Steffen Blaurock; Evamarie Hey-Hawkins
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2001
• Journal issue: 20
• Pages of publication: 3115 - 3118
• a: 34.9726 ± 0.001 Å
• b: 11.5969 ± 0.0003 Å
• c: 28.4498 ± 0.0009 Å
• α: 90°
• β: 115.202 ± 0.002°
• γ: 90°
• Cell volume: 10440.2 ± 0.5 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1239
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for significantly intense reflections: 0.1414
• Weighted residual factors for all reflections included in the refinement: 0.1542
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No