Information card for entry 7011005

Structure parameters

• Formula: C36.5 H49 Cl4 Co F6 N4 Sb
• Calculated formula: C36.5 H46 Cl4 Co F6 N4 Sb
• Title of publication: Cationic 2,6-bis(imino)pyridine iron and cobalt complexes: synthesis, structures, ethylene polymerisation and ethylene/polar monomer co-polymerisation studies
• Authors of publication: George J. P. Britovsek; Vernon C. Gibson; Stefan K. Spitzmesser; Kilian P. Tellmann; Andrew J. P. White; David J. Williams
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1159 - 1171
• a: 25.879 ± 0.005 Å
• b: 10.073 ± 0.002 Å
• c: 36.573 ± 0.004 Å
• α: 90°
• β: 93.011 ± 0.012°
• γ: 90°
• Cell volume: 9521 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1477
• Residual factor for significantly intense reflections: 0.0755
• Weighted residual factors for all reflections: 0.2333
• Weighted residual factors for significantly intense reflections: 0.1783
• Goodness-of-fit parameter for all reflections: 1.005
• Goodness-of-fit parameter for significantly intense reflections: 1.11
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No