Information card for entry 7011015

Structure parameters

• Formula: C36 H32 N8 O22 P2 Pu1.5
• Calculated formula: C36 H32 N8 O22 P2 Pu1.5
• Title of publication: Synthesis and crystal structure of a ten-coordinate plutonium(iv) ion complexed by 2-[(diphenylphosphino)methyl]pyridine N,P-dioxide: [Pu(NO3)3{2-[(C6H5)2P(O)CH2]C5H4NO}2][Pu(NO3)6]0.5
• Authors of publication: Matonic, John H.; Neu, Mary P.; Enriquez, Alejandro E.; Paine, Robert T.; Scott, Brian L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 11
• Pages of publication: 2328
• a: 12.0407 ± 0.0006 Å
• b: 14.2228 ± 0.0007 Å
• c: 15.6363 ± 0.0007 Å
• α: 65.195 ± 0.001°
• β: 80.571 ± 0.001°
• γ: 72.381 ± 0.001°
• Cell volume: 2314.58 ± 0.19 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0318
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0601
• Weighted residual factors for all reflections included in the refinement: 0.0632
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No