Information card for entry 7011121

Structure parameters

• Formula: C44 H100 Si9
• Calculated formula: C44.0288 H100.072 Si9.0072
• Title of publication: Hexakis(trialkylsilyl)cyclotrisilanes and photochemical generation of bis(trialkylsilyl)silylenes
• Authors of publication: Mitsuo Kira; Takeaki Iwamoto; Toyotaro Maruyama; Tsuyoshi Kuzuguchi; Dongzhu Yin; Chizuko Kabuto; Hideki Sakurai
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 7
• Pages of publication: 1539 - 1544
• a: 18.223 ± 0.002 Å
• b: 15.8148 ± 0.0018 Å
• c: 11.7534 ± 0.0004 Å
• α: 90°
• β: 123.956 ± 0.001°
• γ: 90°
• Cell volume: 2809.6 ± 0.5 ų
• Cell temperature: 150.2 K
• Ambient diffraction temperature: 150.2 K
• Number of distinct elements: 3
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0939
• Weighted residual factors for all reflections included in the refinement: 0.0978
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No