Information card for entry 7011132

Structure parameters

• Formula: C20.5 H33 Cl P2 Pt
• Calculated formula: C20.5 H33 Cl P2 Pt
• Title of publication: Preparation of buta-1,3-diynyl complexes of platinum(II) and their use in the construction of neutral molecular squares: synthesis, structural and theoretical characterisation of cyclo-{Pt(μ-CCCC)(dppe)}4 and related chemistry
• Authors of publication: Michael I. Bruce; Karine Costuas; Jean-François Halet; Ben C. Hall; Paul J. Low; Brian K. Nicholson; Brian W. Skelton; Allan H. White
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 383 - 398
• a: 12.3036 ± 0.0008 Å
• b: 12.3036 ± 0.0008 Å
• c: 16.455 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2490.9 ± 0.3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 137
• Hermann-Mauguin space group symbol: P 42/n m c :2
• Hall space group symbol: -P 4ac 2a
• Residual factor for all reflections: 0.032
• Residual factor for significantly intense reflections: 0.017
• Weighted residual factors for all reflections: 0.036
• Weighted residual factors for all reflections included in the refinement: 0.034
• Goodness-of-fit parameter for all reflections: 1.234
• Goodness-of-fit parameter for all reflections included in the refinement: 1.366
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No