Information card for entry 7011134

Structure parameters

• Formula: C140 H156 O10 P8 Pt4 S10
• Calculated formula: C140 H156 O10 P8 Pt4 S10
• Title of publication: Preparation of buta-1,3-diynyl complexes of platinum(II) and their use in the construction of neutral molecular squares: synthesis, structural and theoretical characterisation of cyclo-{Pt(μ-CCCC)(dppe)}4 and related chemistry
• Authors of publication: Michael I. Bruce; Karine Costuas; Jean-François Halet; Ben C. Hall; Paul J. Low; Brian K. Nicholson; Brian W. Skelton; Allan H. White
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 383 - 398
• a: 13.127 ± 0.002 Å
• b: 17.201 ± 0.003 Å
• c: 17.57 ± 0.003 Å
• α: 70.582 ± 0.003°
• β: 68.705 ± 0.003°
• γ: 87.309 ± 0.003°
• Cell volume: 3473.8 ± 1 ų
• Cell temperature: 153 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.103
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for all reflections: 0.084
• Weighted residual factors for all reflections included in the refinement: 0.069
• Goodness-of-fit parameter for all reflections: 1.917
• Goodness-of-fit parameter for all reflections included in the refinement: 1.938
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No