Information card for entry 7011159

Structure parameters

• Formula: C48.25 H44.5 F6 O0.75 P3 Rh S2 W
• Calculated formula: C48.25 H44.5 F6 O0.75 P3 Rh S2 W
• Title of publication: Syntheses and reactivities of hydrosulfido- or sulfido-bridged heterobimetallic complexes containing Group 6 and Group 9 metals
• Authors of publication: Hiroko Kato; Hidetake Seino; Yasushi Mizobe; Masanobu Hidai
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 7
• Pages of publication: 1494 - 1499
• a: 11.005 ± 0.002 Å
• b: 36.622 ± 0.002 Å
• c: 12.02 ± 0.002 Å
• α: 90°
• β: 98.06 ± 0.01°
• γ: 90°
• Cell volume: 4796.5 ± 1.2 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 8
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.04
• Residual factor for significantly intense reflections: 0.04
• Weighted residual factors for significantly intense reflections: 0.0377
• Weighted residual factors for all reflections included in the refinement: 0.0377
• Goodness-of-fit parameter for all reflections included in the refinement: 1.415
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No