Information card for entry 7011203

Structure parameters

• Formula: C152 H260 O16 P4 Pd4 S8 Zr4
• Calculated formula: C152 H260 O16 P4 Pd4 S8 Zr4
• Title of publication: Early/late heterobimetallics: unusual tetranuclear Zr/Ni and octanuclear Zr/Pd complexes with bridging bifunctional sulfidoacetato ligands
• Authors of publication: Barbara Wenzel; Peter Lönnecke; Matthias Stender; Evamarie Hey-Hawkins
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 478 - 480
• a: 13.3846 ± 0.0015 Å
• b: 18.954 ± 0.002 Å
• c: 21.79 ± 0.002 Å
• α: 108.654 ± 0.002°
• β: 104.881 ± 0.002°
• γ: 92.592 ± 0.002°
• Cell volume: 5012.7 ± 0.9 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1456
• Residual factor for significantly intense reflections: 0.0829
• Weighted residual factors for significantly intense reflections: 0.2458
• Weighted residual factors for all reflections included in the refinement: 0.2931
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No