Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7011210
Preview
Coordinates | 7011210.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H45 K O10 |
---|---|
Calculated formula | C25 H45 K O10 |
Title of publication | Ether and crown ether adduct complexes of sodium and potassium cyclopentadienide and methylcyclopentadienide—molecular structures of [Na(dme)Cp]∞, [K(dme)0.5Cp]∞, [Na(15-crown-5)Cp], [Na(18-crown-6)CpMe] and the “naked Cp−” complex [K(15-crown-5)2][Cp] |
Authors of publication | Marcus L. Cole; Cameron Jones; Peter C. Junk |
Journal of publication | J. Chem. Soc., Dalton Trans. |
Year of publication | 2002 |
Journal issue | 6 |
Pages of publication | 896 - 905 |
a | 8.793 ± 0.003 Å |
b | 9.119 ± 0.003 Å |
c | 9.377 ± 0.003 Å |
α | 84.667 ± 0.006° |
β | 89.76 ± 0.005° |
γ | 78.841 ± 0.007° |
Cell volume | 734.4 ± 0.4 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1244 |
Residual factor for significantly intense reflections | 0.0825 |
Weighted residual factors for significantly intense reflections | 0.2144 |
Weighted residual factors for all reflections included in the refinement | 0.2506 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.984 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7011210.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.