Information card for entry 7011312

Structure parameters

• Formula: C65 H86 N8 O18 Zn4
• Calculated formula: C65 H76 N8 O18 Zn4
• Title of publication: Zinc(II) complexes of tetrapodal ligands derived from tetra-substituted 1,n-diaminoalcohols
• Authors of publication: Harry Adams; Darren Bradshaw; David E. Fenton
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 925 - 930
• a: 20.929 ± 0.005 Å
• b: 19.961 ± 0.005 Å
• c: 18.994 ± 0.005 Å
• α: 90°
• β: 90 ± 0.004°
• γ: 90°
• Cell volume: 7935 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2725
• Residual factor for significantly intense reflections: 0.0927
• Weighted residual factors for significantly intense reflections: 0.2453
• Weighted residual factors for all reflections included in the refinement: 0.312
• Goodness-of-fit parameter for all reflections included in the refinement: 0.872
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No