Information card for entry 7011386

Structure parameters

• Formula: C34 H85 Ag10 O16.5 P8 Se17
• Calculated formula: C34 H85 Ag10 O16.5 P8 Se17
• Title of publication: Novel silver diselenophosphate clusters: structures of Ag10(µ10-Se)[Se2P(OEt)2]8 and {Ag[Se2P(OPri)2]}6Metal dialkyl diselenophosphates. Part 5. For preceding paper see ref. 1.
• Authors of publication: Liu, C. W.; Shang, Iu-Jie; Hung, Chiu-Mine; Wang, Ju-Chung; Keng, Tai-Chiun
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 9
• Pages of publication: 1974
• a: 49.153 ± 0.003 Å
• b: 14.9447 ± 0.0009 Å
• c: 25.306 ± 0.0015 Å
• α: 90°
• β: 107.872 ± 0.001°
• γ: 90°
• Cell volume: 17692.2 ± 1.8 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0917
• Residual factor for significantly intense reflections: 0.0714
• Weighted residual factors for significantly intense reflections: 0.1703
• Weighted residual factors for all reflections included in the refinement: 0.1857
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No