Information card for entry 7011436

Structure parameters

• Formula: C9 H19 Cl2 Co N4 O2
• Calculated formula: C9 H19 Cl2 Co N4 O2
• Title of publication: Polydentate ligand construction: intramolecular condensation reactions in the synthesis of imine-containing ligands
• Authors of publication: Browne, Julian M. W.; Wikaira, Jan; Fitchett, Christopher M.; Hartshorn, Richard M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 10
• Pages of publication: 2227
• a: 8.966 ± 0.004 Å
• b: 14.474 ± 0.007 Å
• c: 10.343 ± 0.005 Å
• α: 90°
• β: 98.319 ± 0.007°
• γ: 90°
• Cell volume: 1328.1 ± 1.1 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0312
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for significantly intense reflections: 0.0709
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No